Allylamine → HCID 20395266, compound

Participants

Reaction Steps

42.4 g of 4A and 38 g of 2-propenamine were mixed in 165 ml of ethanol and the mixture was stirred at room temperature for 90 hours. The solvent was removed under reduced pressure. The residue was partitioned between ether and water. The ether solution was dried (MgSO4), about half the solvent was evaporated, and solid which formed was filtered, then dried under reduced pressure to give 4, mp: 113°-115° C.

Provenance & Evidence