HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-chloro-3-oxopropionate → HCID 54284815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-chloro-3-oxopropionate | HCID 118931 | — |
| Reactant | N-benzyl-5-chloro-2-nitroaniline | HCID 2867656 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54284815 | HCID 54284815 | — |
Reaction Steps
52 g of N-benzyl-N-(2-nitro-5-chlorophenyl) amine and 35.5 g of (chloroformyl)acetic acid ethyl ester in 500 ml benzene are refluxed for 15 hours. The reaction is cooled, washed with dilute aqueous sodium bicarbonate, dried and the solvent evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04164580 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-3ebf8048fffd400b92fe438032692ede |
| Source note | uspto-grants-1979_08 |