反应详情

One equivalent of 4-allyl-3-methyl-2,6-dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.

1. temperatureThe mixture is refluxed for 5 hours
2. washThe organic phase is washed with 5% hydrochloric acid
3. dry with materialwater, dried over calcium sulfate
4. customremoved in vacuo
5. customto leave the above-named product