HRID261300

反应详情

EQUATION

反应方程式

HRID 261300 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of methyl 2- methyl-5-nitrobenzyl ether (12 g. 0.066 M), methoxyacetone [20 g (used as solvent)], 2-naphthalenesulfonic acid (0.3 g) and 5% Pt/C (0.7 g) is shaken on a Parr hydrogenator maintaining the temperature below 40° with external cooling. The theoretical amount of hydrogen (0.26 M) is consumed and further uptake ceases after 2 hours.

WORKUP

后处理

  1. temperaturemaintaining the temperature below 40° with external cooling
  2. customThe theoretical amount of hydrogen (0.26 M) is consumed