HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2,3-dihydroxypropionyl)-3-amino-5-nitroaniline → HCID 178467278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2,3-dihydroxypropionyl)-3-amino-5-nitroaniline | HCID 20394926 | — |
| Reactant | 3,5-Diacetyl-2,6-dihydroxy-4h-pyran-4-one | HCID 135465969 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178467278 | HCID 178467278 | 42.9% |
Reaction Steps
A mixture of 785 mg (3.3 mmole) of N-(2,3-dihydroxypropionyl)-3-amino-5-nitroaniline and 690 mg (3.3 mmole) of 3,5-diacetyl-4,6-dihydroxy-2H-pyran-2-one in 30 ml of methanol was heated under reflux for 30 minutes. After cooling, the crystalline product was filtered and dried in vacuum to give 616 mg of 5-acetyl-4-hydroxy-3-[1-(3-glyceroylamino-5-nitrophenylamino)ethylidene]-2H-pyran-2,6(3H)-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04165365 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-ae0c70339a8842b996e0a8016d577a60 |
| Source note | uspto-grants-1979_08 |