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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 26141Generated: October 25, 2026

Beta-Nitrostyrene → alpha-(Nitromethyl)benzyl diethyldithiocarbamate

https://huagongshe.com/reaction/26141

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBeta-NitrostyreneHCID 7626—
ReactantDiethylammonium diethylcarbamodithioateHCID 2735004—
SolventCarbon DisulfideHCID 6348—
Productalpha-(Nitromethyl)benzyl diethyldithiocarbamateHCID 21324593—

Reaction Steps

As in Example 17, reaction of β-nitrostyrene with diethylammonium diethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)benzyl diethyldithiocarbamate melting at 81° C.-82.5° C. when recrystallized without heating from acetone-2-propanol solution.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04148795
Source datasetuspto-grants-1979_04
ORD IDord-021db1f139f940299dd9a715ed39cc5e
Source noteuspto-grants-1979_04