HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → alpha-(Nitromethyl)benzyl dimethyldithiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Beta-Nitrostyrene | HCID 7626 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | alpha-(Nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324598 | — |
Reaction Steps
Similarly, gradual addition of dimethylamine (45.1 grame, 1 mole) to a methanol solution of carbon disulfide (83.6 grams, 1.1 mole) and β-nitrostyrene (149.1 grams, 1 mole) at 10° C.-30° C. yields α-(nitromethyl)benzyl dimethyldithiocarbamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04148795 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-98e2088458ec45f49bdde01b01fe530b |
| Source note | uspto-grants-1979_04 |