HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3,7-Diaminoheptan-2-one dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,7-Dibenzamidoheptan-2-one | HCID 12769838 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3,7-Diaminoheptan-2-one dihydrochloride | HCID 12769839 | 65% |
Reaction Steps
Crude 3,7-dibenzamidoheptan-2-one (123 g, 0.35 mol) was hydrolysed by heating under reflux with concentrated HCl for 18 hours to give 3,7-diaminoheptan-2-one dihydrochloride (49 g, 65%), m.p. 160°-166° (MeCN). δ(60 MHzD2O) 4.3 (t,CH), 3.1 (t,NHC2), 2.35 (s,CH3), 1.7 (m(CH2)3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166184 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-bea564ca40ea4bc396e0ce96b0366c93 |
| Source note | uspto-grants-1979_08 |