Hydroxylamine → HCID 178525220, compound

HRID 261730Notes

Reaction equation

HRID 261730 reaction equation
[NH2:1][OH:2].[C:3]12([CH2:15][C:14](=[O:16])[O:13][C:11](=[O:12])[CH2:10]1)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]2>>[OH:2][N:1]=[C:11]([OH:12])[CH2:10][C:3]1([CH2:15][C:14]([OH:13])=[O:16])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1

Participants

3

Reactant 2

HCID 787HydroxylamineHCID 45156304HCID 45156304, compound

Product 1

HCID 178525220HCID 178525220, compound

Procedure

In a manner analogous to that described in Example 1, by the reaction of hydroxylamine with 1,1-cycloheptane-diacetic anhydride, there was obtained 1,1-cycloheptane-diacetic acid N-hydroxylimide (m.p. 90°-100° C.) which, by acylation with benzene-sulphonyl chloride, was converted into benzene-sulphonyloxy-1,1-cycloheptane, diacetic acid imide (m.p. 130°-133° C.).

Sources & evidence

ORD record
ord-b4a4c72806a241f591105f47bf5a1e1a
Source dataset
uspto-grants-1979_05
Patent number
US04152326

Reaction notes

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