Triethylamine → HCID 21319860, compound

HRID 262050Notes

Reaction equation

HRID 262050 reaction equation
Cl.[O:2]=[C:3]1[C:9]2[S:10][CH:11]=[CH:12][C:8]=2[CH:7]([NH2:13])[CH2:6][CH2:5][CH2:4]1.[CH3:14][N:15]=[C:16]=[O:17].C(N(CC)CC)C>C(Cl)Cl>[CH3:14][NH:15][C:16]([NH:13][CH:7]1[C:8]2[CH:12]=[CH:11][S:10][C:9]=2[C:3](=[O:2])[CH2:4][CH2:5][CH2:6]1)=[O:17]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 12228Methyl IsocyanateHCID 213198445,6,7,8-tetrahydro-8-oxo-4H-cyclohepta[b]thiophen-4-amine hydrochloride

Product 1

HCID 21319860HCID 21319860, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Stoichiometric quantities of 5,6,7,8-tetrahydro-8-oxo-4H-cyclohepta[b]thiophen-4-amine hydrochloride, methyl isocyanate, and triethylamine are allowed to react in dry methylene chloride to afford the title compound.

Sources & evidence

ORD record
ord-f8f179cbd9834a2287b09274698bcf8f
Source dataset
uspto-grants-1979_05
Patent number
US04153611

Reaction notes

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