HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 4-(4-Methoxystyryl)benzyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 1-(Bromomethyl)-4-[(4-methoxyphenyl)methyl]benzene | HCID 12463848 | — |
| Reactant | 4-(4-Methoxystyryl)benzyl alcohol | HCID 54497926 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-(4-Methoxystyryl)benzyl bromide | HCID 53959967 | — |
Reaction Steps
4-(4-Methoxystyryl)benzyl bromide was prepared from 55 g. of 4-(4-methoxystyryl)benzyl alcohol and hydrogen bromide in 750 ml. of methylene dichloride according to the procedure of Example 1, part (e); yield 50 g., m.p. 147°-148° C. when recrystallized from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04153719 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-e04a4446053944d6a941e588f31addab |
| Source note | uspto-grants-1979_05 |