HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 21318676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21318680 | HCID 21318680 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21318676 | HCID 21318676 | — |
Reaction Steps
Equivalent amounts of 4,5,6,7-tetrahydrobenzo[b]thiophen-7-amine hydrochloride, triethylamine, and ethyl isocyanate in methylene chloride are stirred at room temperature for an hour and then heated to reflux for half an hour. The product is collected, washed well with water, and dried to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154740 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-6a571396d37945598b082d1038a8df89 |
| Source note | uspto-grants-1979_05 |