Triethylamine → HCID 21318669, compound

Participants

Reaction Steps

A mixture of methoxyamine hydrochloride (5 g.) in 60 ml. of methylene chloride is stirred and 6 g. of triethylamine in 15 ml. of methylene chloride is added slowly. After half an hour of stirring, 5.4 g. of 4,5,6,7-tetrahydrobenzo[b]thien-7-yl isocyanate is added dropwise. The mixture is stirred at room temperature for an hour and filtered. The filter cake is washed with water and dried to afford the title compound.

Provenance & Evidence