HCID 21318933, compound → HCID 21318912, compound

Participants

Reaction Steps

α1 -[[[1,1-Dimethyl-2-(methylphenylamino)ethyl]amino]methyl]-4-phenylmethoxy-1,3-benzenedimethanol (1.3 g) in ethanol (60 ml) was hydrogenated over 10% palladium on charcoal (250 mg). The catalyst was filtered off and the filtrate was evaporated to an oil which foamed under high vacuum. The product crystallised as a white microcrystalline powder from dry ether (630 mg) m.p. 131°-133°.

Provenance & Evidence