HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 54140063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 54024227 | HCID 54024227 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54140063 | HCID 54140063 | — |
Reaction Steps
A solution of 1-[3-[[(ethylthio)thiocarbonyl]thio]propanoyl]-L-proline in ethyl acetate is treated with an ethereal solution of diazomethane until persistent yellow color. After discharging the yellow color with a few drops of acetic acid, the solvents are removed in vacuo to yield 1-[3-[[(ethylthio)thiocarbonyl]thio]propanoyl]-L-proline methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154840 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-21a3633d16ab4f6993fd76f4d3a0f7d8 |
| Source note | uspto-grants-1979_05 |