Potassium Carbonate → HCID 178433288, compound

HRID 262594Notes

Reaction equation

HRID 262594 reaction equation
C(=O)([O-])[O-].[K+].[K+].Cl.Cl.[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]>O>[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 30159992-(((5-Methyl-1H-imidazol-4-yl)methyl)thio)ethylamine dihydrochloride

Product 1

HCID 178433288HCID 178433288, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Potassium carbonate (7.75 g.) was added to a solution of 4-methyl-5-[(2-aminoethyl)thiomethyl]-imidazole dihydrochloride (14.6 g.) in water (120 ml.). The solution was stored at room temperature for 15 minutes, then evaporated to dryness, extracted with isopropyl alcohol and the extracts are concentrated to dryness to give 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole.

Workup

  1. customevaporated to dryness
  2. extractionextracted with isopropyl alcohol
  3. concentrationthe extracts are concentrated to dryness

Sources & evidence

ORD record
ord-7f06eb896af94839b98e6ed32fee1922
Source dataset
uspto-grants-1979_05
Patent number
US04154844

Reaction notes

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