HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 1-[2-(Dimethylamino)ethyl]-1,4-cyclohexadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N,N-Dimethylphenylethylamine | HCID 25125 | — |
| Reactant | Lithium | HCID 3028194 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-[2-(Dimethylamino)ethyl]-1,4-cyclohexadiene | HCID 12228920 | — |
Reaction Steps
45 g. (0.3 moles) of the dimethylphenethylamine is reduced by treatment with 16 g. of lithium (2.3 g. atom) in 1.5 l. of ammonia and 250 ml. of ethanol according to the procedure of Example 1(a) to yield crude 1-[2-(dimethylamino)ethyl]-1,4-cyclohexadiene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04149001 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-d981f93023c54880b523e533bbef7a0b |
| Source note | uspto-grants-1979_04 |