HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 54549235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 53687196 | HCID 53687196 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54549235 | HCID 54549235 | — |
Reaction Steps
A mixture of the product of Step (b) (XXXII) (0.005 m), ethyl iodide (0.006 m) and potassium carbonate (2 g) in 20 ml of acetonitrile is heated at reflux for 18 hours. The mixture is then filtered and the filtrate is concentrated. The residue is treated with water and extracted with ethyl acetate. The extracts are dried (Na2SO4) and concentrated to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154932 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-86afa96786424ce38294b3a59cb94024 |
| Source note | uspto-grants-1979_05 |