HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 44279963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 21318818 | HCID 21318818 | — |
| Product | HCID 44279963 | HCID 44279963 | — |
Reaction Steps
A solution of 3.0 g. of t-butyl ethyl p-(hexadecylamino)benzoylmalonate in 10 ml. of trifluoroacetic acid is warmed with stirring for 3 hours. The solution is poured onto ice and neutralized with potassium hydroxide. The resulting precipitate is washed with water and dried. Recrystallization from chloroform gives the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154756 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-0fbc55391f1a4f71a7ed65766bd2a5d7 |
| Source note | uspto-grants-1979_05 |