HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Phenylmethylene)-1-dodecanamine → N-Benzyldodecan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Phenylmethylene)-1-dodecanamine | HCID 89283 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-Benzyldodecan-1-amine | HCID 232909 | — |
Reaction Steps
1.9 g (0.05 mol.) of lithium aluminum hydride was dissolved in 80 ml of anhydrous tetrahydrofuran. N-benzylidene-n-dodecylamine was gradually added to the mixture at room temperature and heated at 50°~60° C. for an hour to yield N-benzyl-n-dodecylamine (III). The product was purified by distillation. b.p. 150°~157° C./0.6 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04155872 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-5cf654d0bbcf46f681d5ca41f05cd851 |
| Source note | uspto-grants-1979_05 |