HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 20298677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | HCID 20298674 | HCID 20298674 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20298677 | HCID 20298677 | 83% |
Reaction Steps
2-[3-(Dimethylamino)propoxy]-5-methoxybenzaldehyde (33.5 g) and 17.4 g of phenethylamine are reacted in 140 ml of toluene following the procedure described in Example 1B yielding 39.9 g of the title compound, boiling point 197°-202° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156079 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-ccb7a478b5f94a348865c0ef7b3fc992 |
| Source note | uspto-grants-1979_05 |