HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → 1-Hydroxy-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 4-Isocyanato-4,5,6,7-tetrahydro-1-benzothiophene | HCID 20537301 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 1-Hydroxy-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea | HCID 20348966 | — |
Reaction Steps
The above compound is prepared in the manner described in Example 6, by allowing 4,5,6,7-tetrahydrobenzo[b]thien-4-yl isocyanate to react with hydroxylamine hydrochloride in the presence of triethylamine. The product melts at 158.5° C. to 160.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156670 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-9d55d1c2b574410f9fa71b6f15058828 |
| Source note | uspto-grants-1979_05 |