Dimethylamine → HCID 70607993, compound

Participants

Reaction Steps

A mixture of 18.8 (0.10 mol) of trans-3a, 4,9,9a-tetrahydronaphtho[2,3-b]furan-2(3H)-one, 35 ml of anhydrous dimethylamine, and 35 ml of dry THF is heated in a small Parr bomb at 100° for 3 days. The cooled reaction mixture is then taken to dryness in vacuo, and the residue triturated with ether to give 22.5 g (97%) of crystalline solid after drying in vacuo.

Provenance & Evidence