HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 21316288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | 4,7,13,16-Tetraoxa-1,10,21,24-tetraazabicyclo[8.8.8]hexacosane | HCID 13810959 | — |
| Product | HCID 21316288 | HCID 21316288 | — |
Reaction Steps
In a manner similar to that described in Example 7, treat 4,7,13,16-tetraoxa-1,10,21,24-tetraazabicyclo[8,8,8]-hexacosane (compound of Example 68B) with methyl chlorocarbonate Isolate and purify the resultant product in a manner similar to that described in Example 7 to obtain 21,24-dicarbomethoxy-4,7,13,16-tetraoxa-1,10,21,24-tetraazabicyclo[8,8,8]hexacosane, m.p. =86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156683 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-94b34a6681d44a3e9e806366c72f8af7 |
| Source note | uspto-grants-1979_05 |