Phthalimide → HCID 86733622, compound

HRID 263280Notes

Reaction equation

HRID 263280 reaction equation
[Br-].[Br-].[CH2:3]([OH:18])[CH2:4][O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][O:14][CH2:15][CH2:16][OH:17].[C:19]1(=[O:29])[NH:23][C:22](=[O:24])[C:21]2=[CH:25][CH:26]=[CH:27][CH:28]=[C:20]12.[OH-].[K+]>C(O)C>[C:19]1(=[O:29])[NH:23][C:22](=[O:24])[C:21]2=[CH:25][CH:26]=[CH:27][CH:28]=[C:20]12.[C:19]1(=[O:29])[NH:23][C:22](=[O:24])[C:21]2=[CH:25][CH:26]=[CH:27][CH:28]=[C:20]12.[CH2:16]([OH:17])[CH2:15][O:14][CH2:13][CH2:12][O:11][CH2:10][CH2:9][O:8][CH2:7][CH2:6][O:5][CH2:4][CH2:3][OH:18]

Participants

5

Reactant 3

HCID 6809PhthalimideHCID 14797Potassium HydroxideHCID 86733621HCID 86733621, compound

Product 1

HCID 86733622HCID 86733622, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to that described in Example 2B, treat the pentaethylene glycol dibromide with phthalimide and potassium hydroxide in ethanol. Isolate and purify the resultant product in a manner similar to that described to obtain pentaethyleneglycol diphthalimide.

Workup

  1. customIsolate
  2. custompurify the resultant product in a manner similar to

Sources & evidence

ORD record
ord-31f83ee0c4ac44bca24c9ac583e1f172
Source dataset
uspto-grants-1979_05
Patent number
US04156683

Reaction notes

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