HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 4,13-Di-(n-decanoyl)-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Decanoyl chloride | HCID 66982 | — |
| Reactant | Diaza-18-crown-6 | HCID 72805 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4,13-Di-(n-decanoyl)-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane | HCID 537315 | — |
Reaction Steps
In a manner similar to that described in Example 5, treat the cyclic diamine obtained in Example 4 and triethylamine in anhydrous benzene with a solution of n-decanoyl chloride (capryl chloride) in anhydrous benzene. Isolate and purify the resultant product in a manner similar to that described to obtain 4,13-di-(n-decanoyl)-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156683 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-dd84780391b84a739b9ba73542ba3cd7 |
| Source note | uspto-grants-1979_05 |