HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Aminosulfonyl)-4-chlorobenzoyl chloride → HCID 21316568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 2-Ethyl-5-methyl-1-benzofuran | HCID 12416506 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21316568 | HCID 21316568 | — |
Reaction Steps
is obtained as described in Example 1 from 10 g 4-chloro-3-sulfamoylbenzoyl chloride and 6.2 g 2-ethyl-5-methylbenzo[b]furan in the presence of 11.4 g aluminum chloride. Colorless crystals, m.p. 147°-150° C. (from methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156732 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-39cb351c2e9f4aa99473c5ae071b218f |
| Source note | uspto-grants-1979_05 |