HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-1-benzofuran → HCID 21316615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-1-benzofuran | HCID 20263 | — |
| Reactant | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 21316615 | HCID 21316615 | — |
Reaction Steps
is obtained as described in Example 1 from 10.1 g 4-chloro-3-sulfamoylbenzoyl chloride and 5.8 g 2-methylbenzo[b]furan in the presence of 11.4 g aluminum chloride. After evaporation of the extraction agent, the residue is stirred with di-isopropyl ether, and the solids are filtered off. Colorless crystals, m.p. 183° C. (from methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156732 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-6e6283f9cc9748389d130876c2b10792 |
| Source note | uspto-grants-1979_05 |