HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methylindole → 3-(4-Chloro-3-methylsulfamoylbenzoyl)-2-methylindole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methylindole | HCID 7224 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Edukt | 4-Chloro-3-methylsulfamoylbenzoyl chloride | HCID 21316637 | — |
| Lösungsmittel | 1,1-Dichloroethane | HCID 6365 | — |
| Produkt | 3-(4-Chloro-3-methylsulfamoylbenzoyl)-2-methylindole | HCID 21316589 | — |
Reaktionsschritte
is obtained as described in Example 10 a) from 2.68 g 4-chloro-3-methylsulfamoylbenzoyl chloride and 1.3 g 2-methylindole in the presence of 2.7 g aluminum chloride in dichloroethane. Colorless crystals, m.p. 246° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04156732 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-856f65f79d224de5b597eeed591581c6 |
| Quellennotiz | uspto-grants-1979_05 |