HRID263294

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7224

1H-Indole, 2-methyl-

C9H9N

HCID6451240

未命名化合物

HCID21316637

未命名化合物

PRODUCTS

生成物

结构：CNS(=O)(=O)c1cc(C(=O)c2c(C)[nH]c3ccccc23)ccc1Cl

HCID21316589

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6365

1,1-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

is obtained as described in Example 10 a) from 2.68 g 4-chloro-3-methylsulfamoylbenzoyl chloride and 1.3 g 2-methylindole in the presence of 2.7 g aluminum chloride in dichloroethane. Colorless crystals, m.p. 246° C.

WORKUP

后处理

customis obtained