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HRID263296

反应详情

EQUATION

反应方程式

HRID 263296 的结构方程式

REACTANTS

反应物

4
结构：CC(C)O
HCID3776

Isopropanol

C3H8O

结构：Cc1cc2ccccc2n1C
HCID13408

1,2-Dimethylindole

C10H11N

结构：NS(=O)(=O)c1cc(C(=O)Cl)ccc1Cl
HCID3017979

4-Chloro-3-sulfamoylbenzoyl chloride

C7H5Cl2NO3S

结构：[Al+3].[Cl-].[Cl-].[Cl-]
HCID6451240

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(C(=O)c2ccc(Cl)c(S(N)(=O)=O)c2)c2ccccc2n1C
HCID21316638

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(Cl)Cl
溶剂HCID6365

1,1-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

is obtained as described in Example 10 (a) from 10 g 4-chloro-3-sulfamoylbenzoyl chloride and 6.53 g 1,2-dimethylindole in dichloro-ethane in the presence of 12 g aluminum chloride. After treatment with isopropanol, crystals having a melting point of 247°-249° C. are obtained.

WORKUP

后处理

  1. customis obtained
  2. customare obtained