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HRID 263314作成日:2026年10月25日

Urea → Heptadecyl carbamate

https://huagongshe.com/reaction/263314

反応式

関与物質

役割名称HCID仕込み量
反応物UreaHCID 1176—
反応物1-HeptadecanolHCID 15076—
触媒NickelHCID 935—
生成物Heptadecyl carbamateHCID 1937254994%

反応手順

A mixture of 256 parts of heptadecyl alcohol, 60 parts of urea and 5 parts of a cation exchanger which is commercially available under the registered name Amberlite 200 and, having been treated in accordance with Example 1, contains nickel, is heated in a stirred vessel to 140°-145° C., whilst stirring. After filtering off the exchanger whilst the reaction solution is hot, 280 parts of heptadecyl carbamate are obtained. This corresponds to a yield of 94% of theory. The product has a melting point of 53°-54° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04156784
出典データセットuspto-grants-1979_05
ORD IDord-fe91ab106e5b4d84b4b3f5742e1a10df
出典メモuspto-grants-1979_05