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Urea → Heptadecyl carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Urea | HCID 1176 | — |
| 反応物 | 1-Heptadecanol | HCID 15076 | — |
| 触媒 | Nickel | HCID 935 | — |
| 生成物 | Heptadecyl carbamate | HCID 19372549 | 94% |
反応手順
A mixture of 256 parts of heptadecyl alcohol, 60 parts of urea and 5 parts of a cation exchanger which is commercially available under the registered name Amberlite 200 and, having been treated in accordance with Example 1, contains nickel, is heated in a stirred vessel to 140°-145° C., whilst stirring. After filtering off the exchanger whilst the reaction solution is hot, 280 parts of heptadecyl carbamate are obtained. This corresponds to a yield of 94% of theory. The product has a melting point of 53°-54° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04156784 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-fe91ab106e5b4d84b4b3f5742e1a10df |
| 出典メモ | uspto-grants-1979_05 |