HRID263314

反应详情

EQUATION

反应方程式

HRID 263314 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 256 parts of heptadecyl alcohol, 60 parts of urea and 5 parts of a cation exchanger which is commercially available under the registered name Amberlite 200 and, having been treated in accordance with Example 1, contains nickel, is heated in a stirred vessel to 140°-145° C., whilst stirring. After filtering off the exchanger whilst the reaction solution is hot, 280 parts of heptadecyl carbamate are obtained. This corresponds to a yield of 94% of theory. The product has a melting point of 53°-54° C.

WORKUP

后处理

  1. additionhaving been treated in accordance with Example 1
  2. temperatureis heated in a stirred vessel to 140°-145° C.
  3. filtrationAfter filtering off the exchanger whilst the reaction solution