HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → HCID 10936768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | HCID 54390831 | HCID 54390831 | — |
| Product | HCID 10936768 | HCID 10936768 | — |
Reaction Steps
Following the procedure described in Referential Example 4, but using 4-(S)-isopropyl-3-(1-oxo-4-methylpentyl)-2-oxazolidinone (5.17 g), prepared in Referential Example 38, and tert-butyl bromoacetate (18.5 ml) as starting materials, the desired compound (6.16 g), having a m.p. of 143°-144° C. after recrystallization from aqueous methanol, was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05643908 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-c04fe0a0a9e64dd1af2f3ca1e1af9609 |
| Source note | uspto-grants-1997_07 |