Piperidine → HCID 53698819, compound

HRID 263465Notes

Reaction equation

HRID 263465 reaction equation
[CH2:1]([O:8][C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15]([OH:17])=O)=[CH:11][C:10]=1[N+:20]([O-:22])=[O:21])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH:23]1[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]1>>[CH2:1]([O:8][C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15]([N:23]2[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]2)=[O:17])=[CH:11][C:10]=1[N+:20]([O-:22])=[O:21])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 8082PiperidineHCID 54275740HCID 54275740, compound

Product 1

HCID 53698819HCID 53698819, compoundYield 65.3%

Procedure

Following a procedure similar to that described in Example 1, but using 1 g of 4-benzyloxy-3-nitrocinnamic acid and 400 mg of piperidine, 0.8 g of the title compound were obtained, melting at 155°-156° C.

Sources & evidence

ORD record
ord-c67e0e63ddf1479bb02f4f39d6f59359
Source dataset
uspto-grants-1997_07
Patent number
US05643925

Reaction notes

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