HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexanol → 12-Bromododecyl prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexanol | HCID 77970 | — |
| Reactant | 12-Bromo-1-dodecanol | HCID 137895 | — |
| Reactant | 2,3-Difluoro-4'-[6-(acryloyloxy)hexyloxy]biphenyl | HCID 21459498 | — |
| Product | 12-Bromododecyl prop-2-enoate | HCID 13841397 | 75.1% |
Reaction Steps
The same procedure as in the synthesis (a) of Example 2 was repeated except that 44.0 g of 12-bromo-1-dodecanol were used instead of 30 g of 6-bromo-1-hexanol to give 39.8 g (Y., 75.1%) of 12-bromododecyl acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05645760 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-5b5dcec9ed9f4ca092e9d375ad46bed9 |
| Source note | uspto-grants-1997_07 |