HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → n-Butylphosphorodichloridate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | n-Butylphosphorodichloridate | HCID 137039 | — |
Reaction Steps
The desired subtitled compound was prepared substantially in accordance with the procedure detailed in Example 8A, using 1.25 ml (13.5 mmol) of phosphorous oxychloride, 1 g (13.5 mmol) of butanol in 5 ml of carbon tetrachloride to provide a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646111 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-c23a89090afc49b7acec677166ba8df0 |
| Source note | uspto-grants-1997_07 |