HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylaniline → (+/-)-5-(dodecylthio)-alpha-phenyl-N-(2,4,6-trimethoxyphenyl)-2H-tetrazole-2-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylaniline | HCID 32484 | — |
| Reactant | 2,4,6-Trimethoxyaniline | HCID 84271 | — |
| Reactant | (+/-)-5-(dodecylthio)-alpha-phenyl-2H-tetrazole-2-acetic acid | HCID 21469499 | — |
| Reactant | 5-decyl-2H-tetrazole-2-acetic acid | HCID 21469529 | — |
| Product | (+/-)-5-(dodecylthio)-alpha-phenyl-N-(2,4,6-trimethoxyphenyl)-2H-tetrazole-2-acetamide | HCID 21469548 | — |
Reaction Steps
When in the general procedure of Example 88 an appropriate amount of (±)-5-(dodecylthio)-α-phenyl-2H-tetrazole-2-acetic acid was substituted for 5-decyl-2H-tetrazole-2-acetic acid and 2,4,6-trimethoxyaniline was substituted for 2,6-diisopropylaniline, the title compound was obtained, mp 141°-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646170 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-4b485d04e504456cb1d150310c3c314f |
| Source note | uspto-grants-1997_07 |