HRID264733

反应详情

EQUATION

反应方程式

HRID 264733 的结构方程式

PROCEDURE

实验过程

As per the procedure of Example 49, uridine (10 g) was treated with dibutyl tin oxide (10.2 g, 1 eq). The resulting 2',3'-O-dibutylstannylene uridine was treated with iodopropane (8 ml, 2 eq.) at 110° C. as per Example 50 to give a mixture of the 2' and 3' isomers (5.5 g) as a foam.

WORKUP

后处理

  1. customto give
  2. additiona mixture of the 2' and 3' isomers (5.5 g) as a foam