huagongshe.com
HRID264739

反应详情

EQUATION

反应方程式

HRID 264739 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccn([C@@H]2O[C@H](CO)[C@@H](O)[C@H]2O)c(=O)n1
HCID6175

Cytidine

C9H13N3O5

结构：CCCCCBr
HCID8057

1-Bromopentane

C5H11Br

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

PRODUCTS

生成物

1
结构：CCCCCO[C@@H]1[C@H](O)[C@@H](CO)O[C@H]1n1ccc(N)nc1=O
HCID15484895

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

Cytidine (10 g, 0.041 mol), sodium hydride (2.4 g, 1.5 eq), bromopentane (7.6 ml, 1.5 eq.) in DMSO (90 ml) were reacted as per the procedure of Example 71, Step 1 to yield the 2' and 3' isomers as a foam (7.6 g).