HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenyltributyltin → 3,4-Dihydro-7-fluoro-6-(2-fluorophenyl)-1(2H)-naphthalenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenyltributyltin | HCID 15047182 | — |
| Reactant | 3,4-dihydro-7-fluoro-6-trifluoromethylsulfonyloxy-1(2H)-naphthalenone | HCID 19036884 | — |
| Product | 3,4-Dihydro-7-fluoro-6-(2-fluorophenyl)-1(2H)-naphthalenone | HCID 19036879 | 53.2% |
Reaction Steps
Using 1.50 g (4.80 mmol) of 3,4-dihydro-7-fluoro-6-trifluoromethylsulfonyloxy-1(2H)-naphthalenone and 2.22 g (5.78 mmol) of 2-fluorophenyltributyltin, the same reaction as described in Reference Example 1 was carried out to obtain 0.66 g of the above-mentioned compound (yield 53%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646283 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-47c62c4d73124b5c971d0d5371738cdd |
| Source note | uspto-grants-1997_07 |