HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyl(4-fluorophenyl)stannane → 3,4-Dihydro-7-fluoro-6-(4-fluorophenyl)-1(2H)-naphthalenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyl(4-fluorophenyl)stannane | HCID 2737524 | — |
| Reactant | 3,4-dihydro-7-fluoro-6-trifluoromethylsulfonyloxy-1(2H)-naphthalenone | HCID 19036884 | — |
| Product | 3,4-Dihydro-7-fluoro-6-(4-fluorophenyl)-1(2H)-naphthalenone | HCID 19036893 | 61.3% |
Reaction Steps
Using 1.50 g (4.80 mmol) of 3,4-dihydro-7-fluoro-6-trifluoromethylsulfonyloxy-1(2H)-naphthalenone and 1.85 g (4.80 mmol) of 4-fluorophenyltributyltin, the same reaction as described in Reference Example 1 was carried out to obtain 0.76 g of the above-mentioned compound (yield 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646283 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-abbaf749185545a2b6fa2ae9729af714 |
| Source note | uspto-grants-1997_07 |