Indene → HCID 178506815, compound

HRID 264866Notes

Reaction equation

HRID 264866 reaction equation
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[Li:10]CCCC>>[CH:1]1([Li:10])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 7219IndeneHCID 178418339Butyllithium

Product 1

HCID 178506815HCID 178506815, compound

Procedure

Indene was reacted with BuLi to form indenyl lithium, which compound was reacted with methyl iodide to form 1-methylindene. Use was made of: 18.2 grams of indene, 100 ml of n-Buli solution, 22.0 grams of methyl iodide.

Sources & evidence

ORD record
ord-1dea91ec7f524be7920ecd9e17f059d3
Source dataset
uspto-grants-1997_07
Patent number
US05646322

Reaction notes

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