Isobutyryl chloride → HCID 12556919, compound

HRID 26488Notes

Reaction equation

HRID 26488 reaction equation
[CH2:1]([NH:5][C:6]1[O:7][CH:8]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[N:10]=1)[CH2:2][CH2:3][CH3:4].[C:17](Cl)(=[O:21])[CH:18]([CH3:20])[CH3:19]>>[CH2:1]([N:5]([C:6]1[O:7][CH:8]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[N:10]=1)[C:17](=[O:21])[CH:18]([CH3:20])[CH3:19])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 62325Isobutyryl chlorideHCID 122952382-(N-Butylamino)-4-phenyloxazole

Product 1

HCID 12556919HCID 12556919, compound

Procedure

2-(N-butylamino)-4-phenyloxazole was acylated with isobutyryl chloride as described in Example 9. An almost colourless oil was obtained on distillation. WT.= 4.9 g., b.p. 140° C. (air-bath temperature)/1 mm., 80%.

Workup

  1. customAn almost colourless oil was obtained on distillation

Sources & evidence

ORD record
ord-f68a0d3dcc1d44c080a26dc4ec867ca8
Source dataset
uspto-grants-1979_04
Patent number
US04150143

Reaction notes

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