HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 21323498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 3-Methylthio-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323426 | — |
| Product | HCID 21323498 | HCID 21323498 | — |
Reaction Steps
3-Methylthio-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine was treated with potassium hydroxide and the reaction mixture was treated as described. This procedure provided 2,11-dihydro-11-phenyl-3H-s-triazolo[3,4-b][3]benzazepin-3-one as crystals. Colorless needles (as recrystallized from methanol), m.p. 258°-260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-5e696d5e7c8a4ba58ff09d9a8575e82b |
| Source note | uspto-grants-1979_04 |