HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylthio-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine → HCID 21323326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylthio-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323426 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 21323326 | HCID 21323326 | — |
Reaction Steps
3-Methylthio-11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine was treated with Raney nickel as described. This procedure provided 11-phenyl-11H-s-triazolo[3,4-b][3]benzazepine as crystals. Colorless prisms (as recrystallized from ethanol), m.p. 217°-218° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-35982f5dd3544393a325bf07f225560f |
| Source note | uspto-grants-1979_04 |