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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 26515Generated: October 30, 2026

m-Chloroperbenzoic acid → HCID 21323323, compound

https://huagongshe.com/reaction/26515

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
Reactant8-methoxy-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepineHCID 21323425—
ProductHCID 21323323HCID 21323323—

Reaction Steps

By a procedure similar to that described in Example 17, 8-methoxy-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine was reacted with m-chloroperbenzoic acid to obtain 8-methoxy-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine. Colorless needles (as recrystallized from chloroform-methanol), m.p. 241°-242° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04150139
Source datasetuspto-grants-1979_04
ORD IDord-a1dca2b110d748d1ae9fbffdc3f3bb94
Source noteuspto-grants-1979_04