HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Diethyl 2-ethoxymethylimidazole-4,5-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl 1-benzyl-2-ethoxymethylimidazole-4,5-dicarboxylate | HCID 19036277 | — |
| Product | Diethyl 2-ethoxymethylimidazole-4,5-dicarboxylate | HCID 19036215 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 42(iv), but using 4.37 g of diethyl 1-benzyl-2-ethoxymethylimidazole-4,5-dicarboxylate [prepared as described in step (i) above], 3.49 g of the hydrochloride of the title compound were obtained as crystals, melting at 60°-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646171 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-ef294745e9ff4dbdaa1dc55a90fc13e3 |
| Source note | uspto-grants-1997_07 |