HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19082160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium peroxymonosulphate | HCID 10313463 | — |
| Reactant | N-[2-(4-Methoxy-2-oxo-3H-1,3-benzothiazol-7-yl)-ethyl]-3-[2-oxo-2-(2-phenylethylamino)ethylthio]propanamide | HCID 19082247 | — |
| Reactant | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 19082160 | HCID 19082160 | — |
Reaction Steps
Potassium peroxymonosulphate (5.57 g) was gradually added to a solution of the compound from step c) (2.81 g) in methanol:water (6:4, 72 ml) cooled to 0°. The mixture was stirred for 4 hours, water added and the whole extracted with chloroform. A yellow solid precipitated from the aqueous layer and was removed by filtration, and washed (water and pentane) to give the subtitled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648370 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-54156872703f46a8b2fd708eb8ff62c2 |
| Source note | uspto-grants-1997_07 |