HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 3,8-dimethoxy-11H-s-triazolo[3,4-b][3]benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 8-methoxy-3-methylsulfonyl-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323419 | — |
| Product | 3,8-dimethoxy-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323416 | — |
Reaction Steps
The reaction of 8-methoxy-3-methylsulfonyl-11H-s-triazolo[3,4-b][3]benzazepine with sodium methoxide yielded 3,8-dimethoxy-11H-s-triazolo[3,4-b][3]benzazepine. Colorless needles (as recrystallized from aqueous methanol), melting point: 185°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-bb3a1619fd494254a6f9b916788ada72 |
| Source note | uspto-grants-1979_04 |